指环胺类固化剂MXDA(间苯二甲胺),1,3-BAC(1,3环己二甲胺)资料及配方参考

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环氧树脂胺类固化剂推荐度：
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脂环胺类固化剂是著名的环氧固化剂,有耐水性好,韧性好,抗化学性能好,粘附性好,粘度低等优点。,1,3-BAC(1,3环己二甲胺)是其中举足轻重的固化剂之一,是多重改性固化剂的原料之一,能同苯乙烯,环氧氯丙烷等改性成温和特效的固化剂。其本身也是一种优良的环氧固化剂。MXDA(间苯二甲胺)是是BAC的相似物,因为苯环同脂环的区别,效果有一定的不同。

Epoxy Hardenerd Raw Materialil

MXDA & 1,3‐BAC (2)

recommended formulation

Technical Data

Sheet

ContactInformation中国

上海菱晓贸易有限公司

北京分公司李功

地址：北京市朝阳区东三环中路12号现代柏利大厦1008室电话： 010-8454 9884 / 139 1195 4356 传真：010-8454 9863

1. MXDA, 1,3MXDA13‐BAC showshow…shorter drying time(Source: TSR10081H‐OHP)

MXDA

EpoxyResin

Formulation

Hardener

jER828

(BisAType Epoxy)(EEW 186)

(13500mPa s/25℃)

1,3‐BAC100g19g9.1mPa s35635.677min

IPDA100g22g18mPa s42642.6205min

D‐230100g32g9mPa s60060.0521min

(300g)

100g18g6.8mPa s34034.0132min

AmineViscosity (25℃)

AHEW

PropertyPot Life (23℃, 50g)

MXDA

Set to touch

RCI drying

time(hr:min)

Dust free

Dry through

2:004:30>24:00

1,3‐BAC1:454:30>24:00

IPDA4:009:00>24:00

D‐2309:3015:3021:30

MXDA

Set to touch

RCI drying time(hr:min)

Dust freefDry through

13:30>24:00>24:00

1,3‐BAC13:00>24:00>24:00

IPDA21:00>24:00>24:00

D‐230>24:00>24:00>24:00

2. (Source: TSR4109H)

OH2H

SalicylicAcid

「MXDA/BA/SA//」,「1,3,‐BAC/BA/SA//」systemy show…shorter drying time, good propertyMXDA ‐S

py ResinEpoxy

jER828

(BiAType)(EEW(BisAT)(EEW 190)

1,3‐BAC ‐S100gg18.7g19.8g2.8g－798min

IPDA ‐S100gg22.4g19.8g2.8g110mPa s

8521min

100gg17.9g19.8g2.8g62mPa s7715min

Amine

Formulation

Hardener

Benzyl AlcoholSalicylicAcidViscosity (25℃)

AHEW

Property

Pot Life (23℃, 50g)

MXDA ‐S

Set to touch

RCI drying time

(hr:min)

Dust freeDry through

Appearance (7days)

Pencil hardness

1 / 4 / 7 days

★

2:003:005:00★

★

1,3‐BAC ‐S1:303:104:30★

★

IPDA ‐S2:006:009:00★

★

2H / 2H / 3H

★★★★

★★★

★★★★

2H / 2H / 3H

25★

★

★★★★

H / 2H / 2H

17★★★

★

★★

★

Cross‐hatchhhAdhesiondh

Number of residual squares /25

10%NaOH(aq.)

Chemical Resistance(1week)

10% H2SO4(aq.)Humidity (49℃,98%RH ,2weeeks)Salt Spray 5% NaCl(35℃, 2weeks)

MXDA ‐S

Set to touch

RCI drying time(hr:min)

Dust freeDry through

Appearance (7days)

Pencil hardness

1 / 4 / 7 days

★

4:008:0011:00★

★

1,3‐BAC ‐S23:00>24:00>24:00★

★

IPDA ‐S5:00>24:00>24:00★

★

H / 2H / 2H<6B / <6B / <6B<6B / 4B / B

3. MXDA Adduct (IPDA blend)

(Source: TSR12031H‐OHP)

MXDAAdduct (/IPDA blend) system showsshows…

faster curing, better Appearance, water spotting resistanceMXDAAdduct

Epoxy Resin

jER828(BisAType)

Amine

Formulation

jER828

Hardener

Benzyl AlcoholViscosity (25(℃)

AHEW

100g20.9g14.3g23.4g550mPa s109

IPDA

Adduct100g25.1g9.1g22.8g460mPa s106

MXDA/IPDA= 3/7 Blend

100g6.3g(MXDA)4.3g7.0g

17.6g(IPDA)6.4g16.0g

500mPa s107

MXDAAdduct

RCI drying time

Dust free

★★★★

2:30★★★★

★★★★

IPDAAdduct4:15★★★★H / H / H55min

★★★★

★★★

★★★★

★★

★★★★

MXDA/IPDA= 3/7 Blend

3:15★★★★

★★

★★★★

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1day7days1 / 4 / 7 days

H / H / H25min★★★★

★★★★

H / H / H39min★★★★

★★★★

Pot Life (23℃, 300g)

10%NaOH(aq.)

Chemical Resistance(1week)

10% H2SO4(aq.)

WaterSalt Spray 5% NaCl(35℃,4weeks)

3. MXDA Adduct (IPDA blend)

(Source: TSR12031H‐OHP)

MXDAAdduct (/IPDA blend) system showsshows…

faster curing, better Appearance, water spotting resistanceMXDAAdduct

Epoxy Resin

jER828(BisAType)

Amine

Formulation

jER828

Hardener

Benzyl AlcoholViscosity (25(℃)

AHEW

100g20.9g14.3g23.4g550mPa s109

IPDA

Adduct100g25.1g9.1g22.8g460mPa s106

MXDA/IPDA= 3/7 Blend

100g6.3g(MXDA)4.3g7.0g

17.6g(IPDA)6.4g16.0g

500mPa s107

MXDAAdduct

RCI drying time

Dust free

★★★★

3:00★★★★

★★★★

★★

★★★★

★HB / H / H88minIPDAAdduct10:00★★

★

★★★★

★HB / H / H70minMXDA/IPDA= 3/7 Blend

8:00★★

★★

★

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1day7days1 / 4 / 7 days

F / H / H48min

Pot Life (15℃, 300g)

MXDAAdduct

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1day7days1 / 4 / 7 days

★★★★

★

★★★★

★H/ H / H45minIPDAAdduct★★

★

★★★★

MXDA/IPDA= 3/7 Blend★★★★

★★★★

H / H / H28min

H / H / H40min

Pot Life (30℃, 300g)

4. 1,3‐BAC Adduct (IPDA blend)

(Source: TSR12031H‐OHP)

1,313‐BAC/IPDA adduct system shows…shows

faster curing, water spotting resistance, good yellowing resistance1,3‐BACAdduct

Epoxy Resin

jER828(BisAType)

Amine

Formulation

jER828

Hardener

y AlcoholBenzylViscosity (25℃)

AHEW

100g21.2g11.1g21.5gg420mPa s100

IPDA

100g25.1g9.1g22.8gg460mPa s106

1,3‐BAC/IPDA

2100g4.2g(1,3‐BAC)2.2g4.7gg

20.1g

(IPDA)7.3g18.2gg

450mPa s105

1,3‐BAC

Adduct

RCI drying time

Dust free

★★★★

2:15★★★★

★★★★

★★

★★★★

IPDAAdduct4:15★★★★H / H / H55min★

★★

★★★

18.7

19.7★★★

★★★

★★★★

18.4

★★

★★★★

1,3‐BAC/IPDA= 2/8 Blend

3:45★★★★

★★★★

★★★

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1dayd7days1 / 4 / 7 days

H / H / H23min★★★★

★★★

H / H / H41min★★★

★★★

Pot Life (23℃, 300g)

10%NaOH(aq.)

Chemical

Resistance(1week)

10% H2SO4(aq.)

WaterSalt Spray 5% NaCl(35℃,4weeks)

UVTest(Yellow Index after 600hr)

4. 1,3‐BAC Adduct (IPDA blend)

(Source: TSR12031H‐OHP)

1,313‐BAC/IPDA adduct system shows…shows

faster curing, water spotting resistance, good yellowing resistance1,3‐BACAdduct

Epoxy Resin

jER828(BisAType)

Amine

Formulation

jER828

Hardener

y AlcoholBenzylViscosity (25℃)

AHEW

100g21.2g11.1g21.5gg420mPa s100

IPDA

100g25.1g9.1g22.8gg460mPa s106

1,3‐BAC/IPDA

2100g4.2g(1,3‐BAC)2.2g4.7gg

20.1g

(IPDA)7.3g18.2gg

450mPa s105

1,3‐BAC

Adduct

RCI drying time

Dust free

★★★★

11:30★★★★HB / H / H37min

★★

★★★★

★HB / H / H88minIPDAAdduct10:00★★

★

★★★★

1,3‐BAC/IPDA= 2/8 Blend

8:45★★★★HB / H / H69min

★★

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1day7days1 / 4 / 7 days

Pot Life (15℃, 300g)

1,3‐BACAdduct

Dryness(1day)Appearance (7days)

Water Spotting ResistancePencil hardness

1day7days1 / 4 / 7 days

★★★★

IPDAAdduct★★★★H/ H / H45min

★

1,3‐BAC/IPDA= 2/8 Blend★★★★

★★★★

H / H / H22min

H / H / H36min

Pot Life (30℃, 300g)

5. 1,3‐BAC Adduct (Fast cure at low temp.)

(Source: TSR10051H)

1,3,‐BACAdduct with additives systemy shows…Prevention of surface stickiness at low temp,faster curing, water spotting resistance, colorless1,3‐BACAdduct

Epoxy Resin

jER807 (BisFType )

(EEW 169)(3300mPa s/25℃)

1,3‐BACAdduct+ Additives

100g23.1g12.2g3.9g0.45g0.9g4.5g6400mPa s

100g23.6g12.4g4.0g―――3500mPa s

1,3‐BAC / jER828/ Benzyl Alcohol

Formulation

Hardener

BYK‐345KP‐390TriphenylPhosphiteViscosity (25℃)

AHEW

(BYK‐345; surface modifier of BYK‐chemie, Polyether modified polydimethylsiloxane)(KP‐390; water resistance agent of Shin‐Etsu Chemical, Amino modified silicone)

1,3‐BACAdduct

Set to touch

RCI drying time(hr:min)

Dust freeDry through

Appearance (7days)

16 hours

Dryness

1day4 days7days16 hours

Water Spotting Resistance

1dayy4 days7days

Pencil hardness

1 / 4 / 7 days

★★★★★★★★★

4:0017:00>24:00★★★★★★★★★3B/ HB / HB32min

★★★★★★★★★

Recommended

1,3‐BACAdduct

1:307:00>24:00★★★★★★★★★

★★★★★★★

H / H / H22min

Pot Life (23℃, 50g)

6. 1,3‐BAC Adduct (Long potlife(1) –amine blend)

(Source: TSR06014H)

1,3,‐BACAdduct with D‐400 or IPDA Adduct systemy shows…Longer Potlife, good dryness or water spotting resistance1,3‐BACAdduct

Epoxy Resin

jER828 (BisAType )

(EEW 186)

1,3‐BAC/D‐400=7/3100g17.1g9.0g2.9g12.4gg―710mPa s77

1,3‐BAC/D‐400=5/5100g13.5g7.1g2.3g22.8gg―270mPa s85

1,3‐BAC/IPDA adduct

=5/5

100g9.9g5.2g1.7g―13.1g3.6g3500mPa s62

100g21.3g11.1g3.6g――3500mPa s67

1,3‐BAC / jER828/ Benzyl Alcohol

Formulation

D‐400

Hardener

IPDA/ jER828Viscosity (25℃)

AHEW

1,3‐BACAdduct

Pot Life (23℃, 50g)

Set to touch

RCI drying time(hr:min)

Dust freeDry through

Appearance (7days)

16 hours

Dryness

1day4 days7days16 hours

WaterWt SpottingSttiResistance

1day4 days7days

Pencil hardness

1 / 4 / 7 days

32min1:302:30>24:00★★★★★★★★★★★★★★★★★★★★2H / 2H / 2H

1,3‐BAC/D‐400=7/364min2:005:00>24:00★★★★★★★★★

1,3‐BAC/D‐400=5/5147min4:008:45>24:00

1,3‐BAC/IPDA adduct

=5/564min1:302:30>24:00

★★★★★★★★★★★★★★★★★★★

★★★★★★★★★★★★★★★★★★★★★★★★★★★★

F / H / H

★★★★★★★★HB/ H / H

★★★★★★★★★★★★★★★★

H / H / H

(Pencil Hardness: HB < F < H < 2H)

(Source: PRA

‐92‐03)

MXDA,

1,3

‐BAC (Long potlife(2) –Acrylonitrileadduct

(or

G‐

240))

MXDA/AN,/, 1,3,‐BAC/AN/ Adduct systemy

shows…

Longer Potlife, good

drynessAcrylonitrile

MXDA

EpoxyResin

jER828

(BisAType )(EEW 186)

MN‐1100g20.1g3.9g223mPa s44.6170min

MN‐2100g21.7g6.3g232mPa s52.1270min

MN‐3100g23.7g9.3g245mPa s61.4270min

MN‐4100g28.4g16.6g3100mPa s83.7330min

MN‐5100g32.1g21.9g3155mPa s100>330min

MN‐6100g36.0g28.0g3200mPa s119>330min

100g18.3g―17mPa s34.0130min

MXDA

Formulation

Hardener

AcrylonitrileColor(gardner)Viscosity(25℃)AHEW

Pot Life (20℃, 50g)

1,3‐BAC

EpoxyResin

jER828

(BisAType )(EEW 186)()

BN‐1100g21.1g3.9g125

mPa s46.5100min

BN‐2100g22.7g6.3g137mPa s53.9130min

BN‐3100g24.8g9.2g155mPa s63.2150min

BN‐4100g29.5g16.5g1115mPa s85.6150min

BN‐5100g33.3g21.7g1182mPa s102>150min

BN‐6100g37.2g27.8g1230mPa s121>150min

100g19.1g―19mPa s35.575min

1,3‐BAC

Formulation

Hardener

AcrylonitrileColor(gardner)Viscosity(25℃)AHEW

Pot Life (20℃, 50g)

8. MXDA, 1,3‐BAC based

Potential

hardener (long

potlife)

Modified hardener

by Ketonesystem

showsshows…Potentiality,

Longer

Potlife

ketone

2+2O

2R1

jER828(BisAtype)

H2NNH2

jER828(BisAtype)

+2O

ketone

ACE MEK MIBK MIPK MTBK

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