ASTME1444-94a磁粉检测实践标准 英文版
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Designation: E 1444– 94a
An American National Standard
Standard Practice for
Magnetic Particle Examination1This standard is issued under the xed designation E 1444; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscript epsilon (e) indicates an editorial change since the last revision or reapproval. This specication has been approved for use by agencies of the Department of Defense.
1. Scope 1.1 This practice establishes minimum requirements for magnetic particle examination used for the detection of surface or slightly subsurface discontinuities in ferromagnetic material. This practice is intended as a direct replacement of MIL-STD1949. Guide E 709 can be used in conjunction with this practice as a tutorial. 1.2 The magnetic particle examination method is used to detect cracks, laps, seams, inclusions, and other discontinuities on or near the surface of ferromagnetic materials. Magnetic particle examination may be applied to raw material, billets, nished and seminished materials, welds, and in-service parts. Magnetic particle examination is not applicable to nonferromagnetic metals and alloys such as austenitic stainless steels. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2. Referenced Documents 2.1 The following documents form a part of this standard practice to the extent specied herein. 2.2 ASTM Standards: A 275/A 275M Test Method for Magnetic Particle Examination of Steel Forgings2 A 456 Specication for Magnetic Particle Inspection of Large Crankshaft Forgings2 D 96 Test Methods for Water and Sediment in Crude Oil by the Centrifuge Method (Field Procedure)3 E 543 Practice for Evaluating Agencies that Perform Nondestructive Testing4 E 709 Guide for Magnetic Particle Examination4 E 1316 Terminology for Nondestructive Examinations4 2.3 ASNT Document:This practice is under the jurisdiction of ASTM Committee E-7 on Nondestructive Testing and is the direct responsibility of Subcommittee E07.03 on Liquid Penetrant and Magnetic Particle Methods. Current edition approved Nov. 15, 1994. Published January 1995. Originally published as E 1444– 91. Last previous edition E 1444– 94. 2 Annual Book of ASTM Standards, Vol 01.05. 3 Annual Book of ASTM Standards, Vol 05.01. 4 Annual Book of ASTM Standards, Vol 03.03.1
SNT-TC-1A Recommended Practice and Supplement Magnetic Particle Inspection5 2.4 Society of Automotive Engineers (SAE)-AMS Documents:6 AMS 2300 Premium Aircraft-Quality Steel Cleanliness Magnetic Particle Inspection Procedure7 AMS 2301 Aircraft Quality Steel Cleanliness Magnetic Particle Inspection Procedure7 AMS 2303 Aircraft Qu
ality Steel Cleanliness Martensitic Corrosion Resistant Steels Magnetic Particle Inspection Procedure7 AMS 2641 Magnetic Particle Inspection Vehicle7 AMS 3040 Magnetic Particles, Nonuorescent, Dry Method7 AMS 3041 Magnetic Particles, Nonuorescent, Wet Method, Oil Vehicle, Ready-To-Use7 AMS 3042 Magnetic Particles, Nonuorescent, Wet Method, Dry Powder7 AMS 3043 Magnetic Particles, Nonuorescent, Wet Method, Oil Vehicle, Aerosol Packaged7 AMS 3044 Magnetic Particles, Fluorescent, Wet Method, Dry Powder7 AMS 3045 Magnetic Particles, Fluorescent, Wet Method, Oil Vehicle, Ready-To-Use7 AMS 3046 Magnetic Particles, Fluorescent, Wet Method, Oil Vehicle, Aerosol Packaged7 AMS 5355 Investment Castings7 2.5 Federal Standards:6 FED-STD-313 Material Safety Data Sheets, Preparation and the Submission of8 FED-STD-595 Colors8 2.6 Military Standards:6 MIL-STD-1907 Inspection, Liquid Penetrant and Magnetic Particle Soundness Requirements for Materials, Parts, and Weldments85 Available from American Society for Nondestructive Testing, 1711 Arlingate Plaza, P.O. Box 28518, Columbus, OH 43228-0518. 6 Copies of standards, specications, drawings, and publications required by manufacturers in connection with specication acquisition should be obtained from the contracting activity or as directed by the contracting officer. 7 Available from Society of Automotive Engineers, 400 Commonwealth Drive, Warrendale, PA 15096. 8 Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700 Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS.
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
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MIL-STD-410NondestructiveTestingPersonnelQuali ca-
tionandCerti cation8
MIL-STD-1949MagneticParticleInspection,Methodof8
MIL-STD-2175Castings,Classi cationandInspectionof8
MIL-STD-45662CalibrationSystemsRequirements
MIL-I-83387InspectionProcess,MagneticRubber8
DoD-F-87935Fluid,MagneticParticleInspection,Suspen-
sion(Metric)8
2.7OSHADocument:9
29CFR1910.1200HazardCommunication
2.8DoDContracts—Unlessotherwisespeci ed,theedi-
tionsofthedocumentsthatareDoDadoptedarethoselistedin
theissueoftheDoDISS(DepartmentofDefenseIndexof
Speci cationsandStandards)citedinthesolicitation.
2.9OrderofPrecedence—Intheeventofcon ictbetween
thetextofthispracticeandthereferenceddocumentscited
herein,thetextofthispracticetakesprecedence.
3.Terminology
3.1De nitions—Thede nitionsrelatingtomagneticpar-
ticleexamination,whichappearinTerminologyE1316,shall
applytothetermsusedinthispractice.
3.2De nitionsofTermsSpeci ctoThisStandard:
3.2.1alternatingcurrent(ac)—anelectricalcurrentthat
reversesitsdirectionof owatregularintervals.
3.2.2ambientlight—thevisiblelightlevelmeasuredatthe
specimensurfacewiththeblacklight(s)on.
3.2.3contractingagency—aprimecontractor,subcontrac-
tor,orgovernmentagencyprocuringmagneticparticleinspec-
tionservices.
3.2.4gauss(G)—theunitof uxdensityorinductioninthe
cgselectromagneticunitsystem(1G510 4Tesla(T);inair,
1Gisequivalentto1oersted(Oe),whichequals79.58A/m).
3.2.5headshot—theproductionofcircularmagnetization
bypassingcurrentdirectlythroughthepartbeinginspected,or
centralconductor,whilebeingheldincontactwiththehead
stocksinahorizontalwetmachine.
3.2.6magnetic ux—aconceptualizationofthemagnetic
eldintensitybasedonthelinepatternproducedwheniron
lingsaresprinkledonpaperlaidoverapermanentmagnet.
Themagnetic eldliesinthedirectionofthe uxlinesandhas
anintensityproportionaltothelinedensity.
3.2.7magnetization—theprocessbywhichtheelementary
magneticdomainsofamaterialarepredominantlyalignedin
onedirection.
3.2.8retentivity—theabilityofamaterialtoretainmagne-
tismafterthemagnetizingforcehasbeenremoved.
4.Signi canceandUse
4.1Magneticparticleexaminationconsistsofmagnetizing
theareatobeinspected,applyingsuitablypreparedmagnetic
particleswhiletheareaismagnetized,andsubsequently
interpretingandevaluatinganyresultingparticleaccumula-
9AvailablefromSuperintendentofDocuments,U.S.GovernmentPrinting
Office,Washington,D.C.
20402.tions.Maximumdetectabilityoccurswhenthediscontinuityispositionedperpendiculartothemagnetic ux.Inordertodetectdiscontinuitiesinalldirections,atleasttwomagnetic elds,perpendiculartooneanotherinaplaneparalleltothesurfacebeinginspected,shallbeused,exceptwhenspeci callyexemptedbythecontractingagency.5.GeneralPractice5.1AcceptanceRequirements—Theacceptancerequire-mentsapplicabletothepartorgroupofpartsshallbeincorporatedaspartofthewrittenprocedureeitherspeci callyorbyreferencetootherapplicabledocuments,suchasMIL-STD-1907,containingthenecessaryinformation.Applicabledrawingsorotherdocumentsshallspecifytheacceptancesizeandconcentrationofdiscontinuitiesforthecomponent,withzoningofuniqueareasasrequiredbydesignrequirements.Theseacceptancerequirementsshallbeasapprovedonorasspeci edbythecontractingagency.MethodsforestablishingacceptancerequirementsforlargecrankshaftforgingsarecoveredinSpeci cationA456.MethodsforestablishingrequirementsforsteelforgingsarecoveredinTestMethodA275/A275M.MethodsforclassifyingmetalcastingsaregiveninMIL-STD-2175andAMS5355.MIL-STD-1907pro-videsaclassi cationschemeforferromagneticforgings,cast-ings,extrusions,andweldments.5.1.1Aircraft-QualitySteelCleanliness—Theexaminationofaircraft-qualitysteelforcleanlinessusingmagneticparticleexaminationshallbeasspeci edinAMS2300,2301,or2303asappropriatetothetypeofsteelbeinginspected.However,inspectionofpartsfabricatedfromthismaterialshallbeinaccordancewiththerequirementsofthispractice.5.2PersonnelQuali cation—Personnelperformingexami-nationsinaccordancewiththispracticeshallbequali edandcerti edinaccordancewithASNTPersonnelQuali cationSNT-TC-1AorMIL-STD-410formilitarypurposes,orasspeci edinthecontractorpurchaseorder.5.3AgencyQuali cation—Theagencyperformingthetest-ingorexaminationshallmeet,asaminimum,therequirementsofPracticeE543.5.4WrittenProcedure—Magneticparticleexaminationshallbeperformedinaccordancewithawrittenprocedureapplicabletothepartsorgroupofpartsundertesting.Theprocedureshallbeinaccordancewiththerequirementsandguidelinesofthispractice.Theprocedureshallbecapableofdetectingthesmallestrejectablediscontinuitiesspeci edintheacceptancerequirements.Thewrittenproceduremaybegen-eralifitclearlyappliestoallofthespeci edpartsbeingtestedandmeetstherequirementsofthispractice.Allwrittenproceduresshallbeapprovedbyanindividualquali edandcerti edatLevelIIIformagneticparticleexaminationinaccordancewith5.2.Proceduresshallbesubmittedtothecontractingagencywhenrequested.5.4.1ElementsoftheWrittenProcedure—Thewrittenpro-cedureshallincludeatleastthefollowingelements,eitherdirectlyorbyreferencetotheapplicabledocuments:5.4.1.1Procedureidenti cationnumberandthedateitwaswritten;5.4.1.2Identi cationofthepartstowhichtheprocedure
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applies;thisshallincludethematerialandalloyofwhichthe
partsarefabricated;
5.4.1.3Sequenceofmagneticparticleexaminationasre-
latedtomanufacturingprocessoperation,ifapplicable;
5.4.1.4Identi cationoftestpartsusedforsystemperfor-
manceveri cation(see7.1.2and7.1.3);
5.4.1.5Areasoftheparttobeexamined(includean
illustration–eithersketchorphoto);
5.4.1.6Partpreparationrequiredbeforetesting;
5.4.1.7Directionsforpositioningtheitemwithrespectto
themagnetizingequipment;
5.4.1.8Thetypeofmagnetizingcurrentandtheequipment
tobeused;
5.4.1.9Methodofestablishingthemagnetization(head,
coil,prods,yoke,cablewrap,etc.);
5.4.1.10Directionsofmagnetizationtobeused,theorderin
whichtheyareapplied,andanydemagnetizationproceduresto
beusedbetweenshots;
5.4.1.11Thecurrentlevel,orthenumberofampereturns,to
beusedandthedurationofitsapplication;
5.4.1.12Typeofmagneticparticlematerial(dryorwet,
visibleor uorescent,etc.)tobeusedandthemethodand
equipmenttobeusedforitsapplicationand,forthecaseofwet
particles,theparticleconcentrationlimits;
5.4.1.13Typeofrecordsandmethodofmarkingpartsafter
examination;
5.4.1.14Acceptancerequirements,tobeusedforevaluating
indicationsanddispositionofpartsafterevaluation;and
5.4.1.15Postinspectiondemagnetizationandcleaningre-
quirements.
5.5ExaminationSequence—Whenmagneticparticleex-
aminationisspeci ed,itshallbeperformedafterthecomple-
tionofoperationsthatcouldcausesurfaceornear-surface
defects.Theseoperationsinclude,butarenotlimitedto,
forging,heattreating,plating,passivation,coldforming,weld-
ing,grinding,straightening,machining,andproofloading.
Unlessotherwiseapprovedbythecontractingagencyoras
approvedin6.1.3,productionpartsshallbemagneticparticle
inspectedbeforetheapplicationofanycoatings.Also,parts
heattreatedtoanultimatetensilestrengthof180ksiorhigher
thatareheattreatedandsubsequentlyelectroplatedshallbe
inspectedaftertheelectroplatingoperation.
5.6RecordofExamination—Theresultsofallmagnetic
particleinspectionsshallberecorded.Allrecordedresultsshall
beidenti ed, led,andmadeavailableforreviewbythe
contractingagencyuponrequest.Recordsshallprovidefor
traceabilitytothespeci cpartorlotinspected,andtheyshall
identifytheinspectioncontractororfacilityandtheprocedures
usedintheinspection,thelotsize,andthenumberofparts
accepted.
5.7Lighting:
5.7.1VisibleLight—Visiblelightshallbeusedwhenexam-
iningwithnon uorescentparticles.Theintensityofthevisible
lightatthesurfaceofthepartundergoingexaminationshallbe
maintainedataminimumof100fc(1000lx).Theintensity
measurementshallbeconductedwithasuitableilluminance
meterwithaphotopicspectralresponse.
5.7.1.1AmbientVisibleLight—Unlessotherwisespeci ed, uorescentmagneticparticleexaminationsshallbeperformedinadarkenedareawithamaximumambientvisiblelightlevelof2fc(20lx)measuredatthepartsurface.5.7.1.2SpecialVisibleInternalLightSource—Whenexami-nationsofinternalsurfacesmustbeperformedusingspecialvisiblelightsources,theimageproducedmusthavesufficientresolutiontoeffectivelyevaluatetherequireddiscontinuities.Lightintensityshallbemeasuredattheexpectedworkingdistanceoftheequipment.5.7.2BlackLights—Allblacklightsshallbecheckedattheintervalsspeci edinTable1,andafterbulbreplacement,foroutput.Alongerperiodmaybeusedifaplanjustifyingthisextensionispreparedbythenondestructivetestingfacilityandapprovedbythecontractingagency.Theminimumacceptableintensityis1000µW/cm2atthepartbeingexamined.Blacklightre ectorsand ltersshallbecheckeddailyforcleanlinessandintegrity.Damagedordirtyre ectorsor ltersshallbereplacedorotherwisecorrectedasappropriate.5.7.3InternalPartExamination—Wherelampsarephysi-callytoolargetodirectlyilluminatetheexaminationsurface,speciallightingshallbeused.Internalfeaturessuchasbores,holes,andpassageslessthan0.5in.(12.5mm)nominaldiametershallnotrequiremagneticparticleexaminationunlessotherwisespeci edbythecontractingagency.5.8Materials:5.8.1DryParticleRequirements—DryparticlesshallmeettherequirementsofAMS3040.InapplyingAMS3040,theparticlesshallshowindicationsaslistedinTable2onthetestringspecimenofFig.1usingthefollowingprocedure:5.8.1.1Placeaconductorwithadiameterbetween1and1.25in.(25and31mm)andalengthlongerthan16in.(40cm)throughthecenterofthering.Centertheringonthelengthoftheconductor.Magnetizetheringcircularlybypassingthecurrentspeci ingasqueezebulborothersuitableapplicator,applytheparticlestothesurfaceoftheringwhilethecurrentis owing.Examinetheringwithin1minaftercurrentapplicationunderavisiblelightofnotlessthan100fc(1000lx).Thenumberofholeindicationsshallmeetorexceedthosespeci edinTable2.5.8.2WetParticleRequirements—WetparticlesshallmeettherequirementsofAMS3041,3042,3043,3044,3045,or3046,asapplicable.Inapplyingthesespeci cations,theparticlesshallshowindicationsaslistedinTable2onthetestTABLE1RequiredVeri cationIntervalsItemMaximumTimeBetweenVeri cationLighting:Blacklightintensity1dayAmbientlightintensity1dayVisiblelightintensity1daySystemPerformanceusingthetest1daypieceorringspecimenofFig.1Wetparticleconcentration8hours,oreveryshiftchangeWaterbreaktest1dayWetparticlecontamination1weekEquipmentcalibrationcheck:Gaussmeterreading(Teslameter)zeroPriortoUseGaussmeter(Teslameter)accuracy6monthsAmmeteraccuracy6monthsTimercontrol6monthsQuickbreak6monthsDeadweightcheck6
months
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TABLE2RequiredIndicationsWhenUsingtheRingSpecimen
ofFig.1
ParticlesUsedCentralConductorMinimumNumberof
FWDCAmperageHolesIndicated
Wetsuspension,Fluorescent,or14003
Non uorescent25005
34006
Drypowder14004
25006
3400
7
ringspecimenofFig.1usingthefollowingprocedure:
5.8.2.1Placeaconductorwithadiameterbetween1and
1.25in.(25and31mm)andalengthlongerthan16in.(40cm)
throughthecenterofthering.Centertheringonthelengthof
theconductor.Magnetizetheringcircularlybypassingthe
currentspeci edinTable2throughtheconductor.Applythe
suspensiontotheringusingthecontinuousmethod.Examine
theringwithin1minaftercurrentapplication(examinationof
non uorescentbathsshallbeconductedundervisiblelightof
notlessthan100fc(1000lx);examinationof uorescentbaths
shallbeconductedunderablacklightofnotlessthan1000
µW/cm2).Thenumberofholeindicationsshallmeetorexceed
thosespeci edinTable2.
5.8.3SuspensionVehicles—Thesuspensionvehicleforthe
wetmethodshallbealightpetroleumdistillateconformingto
AMS2641(TypeI)orDoD-F-87935,orasuitablyconditioned
waterthatconformstotherequirementsof5.8.4.When
approvedbythecontractingagency,AMS2641(TypeII)may
beused.The ashpointandviscosityshallbeinaccordance
withtherequirementsofAMS2641orDoD-F-87935.The
background uorescenceofthesuspensionvehicleshallbeless
thanthelimitspeci edinDoD-F-87935.
5.8.4ConditionedWaterVehicle—Whenwaterisusedasa
suspensionvehicleformagneticparticles,itshallbecondi-
tionedsuitablytoprovideforproperwetting,particledisper-
sion,andcorrosionprotection.Properwettingshallbedeter-
minedbyawaterbreaktest(see7.1.4.2).Smoothertest
surfacesgenerallyrequirethatagreaterpercentofwetting
agentbeaddedthanroughsurfaces.Nonionicwettingagents
arerecommended.However,wettingagentadditionsshallbe
controlledinallcasesbypHmeasurementstolimitthe
alkalinityofthesuspensiontoamaximumpHof10.0andthe
aciditytoaminimumpHof6.0.
5.8.5ParticleConcentration—Theconcentrationofpar-
ticlesinthetestbathshallbeasspeci edinthewritten
procedure.Particleconcentrationsoutsideoftherangeof0.1to
0.4mLina100-mLbathsamplefor uorescentparticlesand
1.2to2.4mLfornon uorescentparticlesshallnotbeused
unlessauthorizedbythecontractingagency.Fluorescentpar-
ticlesandnon uorescentparticlesshallnotbeusedtogether.
6.Speci cPractice
6.1PreparationofPartsforTest:
6.1.1PreinspectionDemagnetization—Thepartshallbe
demagnetizedbeforeexaminationifprioroperationshave
producedaresidualmagnetic eldthatmayinterferewiththe
examination.
6.1.2SurfaceCleanlinessandFinish—Thesurfaceofthe
parttobeinspectedshallbeessentiallysmooth,clean,dry,andfreeofoil,scale,machiningmarks,orothercontaminantsorconditionsthatmightinterferewiththeefficiencyoftheinspection.6.1.3Coatings—Magneticparticleexaminationshallnotbeperformedwithcoatingsinplacethatcouldpreventthedetectionofsurfacedefectsinferromagneticsubstrate.Suchcoatingsnormallyincludepaintorchromeplategreaterthan0.003in.(0.08mm)inthicknessandferromagneticcoatingssuchaselectroplatednickelgreaterthan0.001in.(0.03mm)inthickness.Ifcoatingsgreaterthantheselimitsarepresentduringexamination,itmustbedemonstratedthattheminimumrejectablediscontinuitiescanbedetectedthroughthemaxi-mumcoatingthicknessapplied.Whensuchcoatingsarenonconductive,theymustberemovedwhereelectricalcontactistobemade.Inhighstressapplicationswhendetectionof nedefectssuchasgrindingcracksandnonmetallicstringersisrequired,examinationwithcoatingsinplaceshallbeper-formedonlywhenithasbeenveri edthattheminimumrejectablediscontinuitiescanbedetectedinthepresenceofthecoating.6.1.4PluggingandMasking—Unlessotherwisespeci edbythecontractingagency,smallopeningsandoilholesleadingtopassagesorcavitiesthatcouldentraporremaincontami-natedwithinspectionmediashallbepluggedwithasuitablenonabrasivematerialthatcanberemovedreadilyand,inthecaseofengineparts,issolubleinoil.Effectivemaskingshallbeusedtoprotectthosecomponents,suchascertainnonme-tallics,thatmaybedamagedbycontactwiththesuspension.6.2MagnetizationMethods:6.2.1TypesofMagnetizingCurrent—Thetypesofcurrentsusedformagneticparticleexaminationarefull-waverecti edalternatingcurrent(3or1phase),half-waverecti edalternat-ingcurrent,andalternatingcurrent.Theequipmentusedshallful llthemagnetizinganddemagnetizingrequirementsad-equately,asoutlinedherein,withoutdamagetothepartundertesting,andtheyshallincludethenecessaryfeaturesrequiredforsafeoperation.6.2.2PermanentMagnets—Permanentmagnetsarenottobeusedformagneticparticleexaminationunlessspeci callyauthorizedbythecontractingagency.Whenpermanentmag-netsareused,adequatemagnetic eldstrengthshallbeestablishedinaccordancewith7.1.5.4.6.2.3Yokes—Whenusingyokes(electromagneticprobes)formagneticparticleexamination,adequatemagnetic eldstrengthshallbeestablishedinaccordancewith7.1.5.4.6.2.4MagnetizingCurrentApplication—Alternatingcur-rentistobeusedonlyforthedetectionofdefectsopentothesurface.Full-waverecti edalternatingcurrenthasthedeepestpossiblepenetrationandmustbeusedforinspectionfordefectsbelowthesurfacewhenusingthewetmagneticparticlemethod.Half-waverecti edalternatingcurrentisadvanta-geousforthedrypowdermethodbecauseitcreatesapulsatingunidirectional eldthatgivesincreasedmobilitytothepar-ticles.6.2.5MagneticFieldDirections—Discontinuitiesarediffi-culttodetectbythemagneticparticlemethodwhentheymakeananglelessthan45°tothedirectionofmagnetization.Toensurethedetectionofdiscontinuitiesinanydirection,each
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Notes:
NOTE1—Allholediametersare60.005in.(60.01cm).Holenumbers8thru12areoptional.
NOTE2—ToleranceontheDdistanceis60.005in.(60.01).
NOTE3—Alldimensionsare60.03in.(60.08)orasnotedinNotes1and2.
NOTE4—Alldimensionsareininches,exceptasnoted.
NOTE5—MaterialisANSI01toolsteelfromannealedroundstock.
NOTE6—Theringmaybeheattreatedasfollows:Heatto1400to1450°F(760to790°C).Holdatthistemperaturefor1h.Coolatamaximumrateof40°F/hr(22°C/hr)tobelow1000°F(540°C).Furnaceoraircooltoroomtemperature.FinishtheringtoRMS25andprotectfromcorrosion.
FIG.1ANSIKETOSToolSteel
Ring
partmustbemagnetizedinatleasttwodirectionsatright
anglestoeachother.Dependingonpartgeometry,thismay
consistofcircularmagnetizationintwoormoredirections,of
bothcircularandlongitudinalmagnetization,oroflongitudinal
magnetizationintwoormoredirections.Exceptionsnecessi-
tatedbypartgeometry,size,orotherfactorsrequirespeci c
approvalofthecontractingagency.
6.2.6MultidirectionalMagnetization—Multidirectional
magnetizationmaybeusedtoful lltherequirementfor
magnetizationintwodirectionsifitisdemonstratedthatitis
effectiveinallcriticalareas.Arti cial awsthatareetchedor
machined,asshownbyadeviceequaltoFig.2,maybeused
toestablish elddirection.Itisvitallyimportantthatthe eld
intensitybebalancedinalldirectionssothatonedirectiondoes
notoverwhelmanotherdirection.Inusingthismethod,the
particleapplicationmustbetimedsothatthemagnetization
reachesitsfullvalueinalldirectionsduringthetimeparticles
aremobileonthesurfaceundertesting(thatis,thecontinuous
method).
6.2.7DirectMagnetization—Directmagnetizationisac-
complishedbypassingcurrentdirectlythroughthepartunder
testing.Electricalcontactismadetothepartusingheadand
tailstock,prods,clamps,magneticleeches,orbyothermeans.Precautionshallbetakentoensurethattheelectricalcurrentisnot owingwhilecontactsarebeingappliedorremovedandthatexcessiveheatingdoesnotoccurinthecontactarea.Unlessotherwisespeci edbythecontractingagency,prodsshallnotbeusedfortheexaminationofaerospacecomponents( ighthardware)oron nishedsurfaces.6.2.8IndirectMagnetization—Indirectpartmagnetizationusespreformedcoils,cablewraps,yokes, eld ow xtures,oracentralconductortoproduceamagnetic eldofsuitablestrengthanddirectiontomagnetizethepartundertest.6.2.9InducedCurrentMagnetization—Inducedcurrentmagnetization(toroidalorcircumferential eld)isaccom-plishedbyinductivelycouplingaparttoanelectricalcoiltocreateasuitablecurrent owinthepartasillustratedinFig.3.Thismethodisoftenadvantageousonring-shapedpartswithacentralapertureandwithanL/Dratiolessthanthree,espe-ciallywheretheeliminationofarcingorburningisofvitalimportance.6.3MagneticFieldStrength:6.3.1MagneticFieldStrength—Theappliedmagnetic eldshallhavesufficientstrengthtoproducesatisfactoryindica-tions,butitmustnotbesostrongthatitcausesthemaskingofrelevantindicationsbynonrelevantaccumulationsof
magnetic
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Examplesofarti cialshimsusedinmagneticparticle
inspectionsystemveri cation.(Notdrawntoscale.)
Theshimsaremadeoflowcarbonsteel(1005steel
foil).Thearti cial awisetchedormachinedonone
sideofthefoiltoadepthof30%ofthefoilthickness.
Inuse,theshimsare rmlyattachedtothetestpart
(e.g.withtapearoundtheedges)withthe awtoward
thepart.
FIG.2Con gurationofArti cialFlawsandTheir
Designation
particles.Factorsthatdeterminetherequired eldstrength
includethesize,shape,andmaterialpermeabilityofthepart,
thetechniqueofmagnetization,themethodofparticleappli-
cation,andthetypeandlocationofthediscontinuitiessought.
Adequatemagnetic eldstrengthmaybedeterminedbyoneor
acombinationofthreemethods:
6.3.1.1Bytestingpartshavingknownorarti cialdefectsof
thetype,size,andlocationspeci edintheacceptancerequire-
ments;
6.3.1.2ByusingaHalleffectprobegaussmetercapableof
measuringthepeakvaluesofthetangent eld;and
6.3.1.3Byusingtheformulasgivenin6.3.7.1-6.3.7.4.
6.3.2WhenusingaHalleffectprobegaussmeter,tangential-
eldstrengths,measuredonthepartsurface,intherangeof30
to60G(2.4to4.8kAm 1)peakvaluesarenormallyadequate
magnetizationlevelsformagneticparticleexamination.Itis
importanttoensurethat eldstrengthsinthisrangearepresent
inallareastobeinspectedonthepart.
6.3.3MagnetizationCurrentLevels—Thecurrentvalues
givenarepeakcurrentvaluesandareapplieddirectlyto
full-waverecti edcurrent.Forothertypesofcurrent,the
operator’smanualortheequipmentmanufacturershouldbe
consultedtodeterminewhatcorrectionfactor,ifany,istobe
usedtoconvertthemeterreadingtoequivalentpeakcurrents.Theprimarycurrentsetsupanoscillating eld.Thisprimarymagnetic eldinducesacurrentintheringshapedpartundertest.FIG.3ExampleofInducedCurrent
Magnetization6.3.4ProdCurrentLevels—Whenusingprodsonmaterial3 4in.(19mm)inthicknessorless,90to115A/in.ofprodspacing(3.5to4.5A/mm)shallbeused.Formaterialgreaterthan3 4in.(19mm)inthickness,100to125A/in.ofprodspacing(4.0to5.0A/mm)shallbeused.Prodspacingshallnotbelessthan2in.(50mm)orgreaterthan8in.(200mm).Theeffectivewidthofthemagnetizing eldwhenusingprodsisonefourthoftheprodspacingoneachsideofalinethroughtheprodcenters.6.3.5DirectCircularMagnetization—Whenmagnetizingbypassingcurrentdirectlythroughthepart(thatis,usingheadshots),thecurrentshallbefrom300to800A/in.ofpartdiameter(12to32A/mm).Thediameterofthepartshallbetakenasthegreatestdistancebetweenanytwopointsontheoutsidecircumferenceofthepart.Currentswillnormallybe500A/in.(20A/mm)orlower,withthehighercurrents(upto800A/in.)beingusedtoinspectforinclusionsortoinspectlow-permeabilityalloyssuchasprecipitation-hardenedsteels.Fortestsusedtolocateinclusionsinprecipitation-hardenedsteels,evenhighercurrents,upto1000A/in.(40A/mm),maybeused.6.3.6CentralConductorCircularMagnetization—Circularmagnetizationmaybeprovidedbypassingcurrentthroughaconductorthatpassesthroughtheinsideofthepart.Inthiscase,alternatingcurrentistobeusedonlywhenthesolepurposeofthetestistoinspectforsurfacediscontinuitiesontheinsidesurfaceofthepart.Ifonlytheinsideofthepartistobeinspected,thediametershallbethegreatestdistancebetweentwopoints,180degreesapartontheinsidecircum-ference.Otherwise,thediameterisdeterminedasin6.3.5.Thefollowingtwoparagraphscovercentrallylocatedandoffsetcentralconductors:6.3.6.1CentrallyLocatedConductor—Whentheaxisofthecentralconductorislocatednearthecentralaxisofthepart,
the
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samecurrentlevelsasgivenin6.3.5shallapply.
6.3.6.2OffsetCentralConductor—Whentheconductor
passingthroughtheinsideofthepartisplacedagainstaninside
wallofthepart,thecurrentlevelsasgivenin6.3.5shallapply,
exceptthatthediametershallbeconsideredthesumofthe
diameterofthecentralconductorandtwicethewallthickness.
Thedistancealongthepartcircumference(interior)thatis
effectivelymagnetizedshallbetakenasfourtimesthediameter
ofthecentralconductor,asillustratedinFig.4.Theentire
circumferenceshallbeinspectedbyrotatingthepartonthe
conductor,allowingforapproximatelya10%magnetic eld
overlap.
6.3.7LongitudinalMagnetizationUsingCoils—
Longitudinalmagnetizationisoftenaccomplishedbypassing
currentthroughacoilencirclingthepart,orsectionofthepart,
tobetested(thatis,byusingacoilshot).Thisproducesa
magnetic eldparalleltotheaxisofthecoil.Forlowor
intermediate llfactorcoils,theeffective eldextendsa
distanceoneithersideofthecoilcenterapproximatelyequalto
theradiusofthecoil(seeFig.5).Forcablewraporhigh- ll
factorcoils,theeffectivedistanceofmagnetizationis9in.(230
mm)oneithersideofthecoilcenter(seeFig.6).Forparts
longerthantheseeffectivedistances,theentirelengthshallbe
inspectedbyrepositioningthepartwithinthecoil,allowingfor
approximately10%effectivemagnetic eldoverlap.
6.3.7.1LongitudinalMagnetizationwithLow-FillFactor
Coils—Whenthecross-sectionalareaofthecoilistenormore
timesthecross-sectionalareaofthepartbeinginspected,the
productofthenumberofcoilturns,N,andthecurrentin
amperesthroughthecoil,I,shallbeasfollows:
(1)Forpartspositionedtothesideofthecoil:
NI5K
~610%!(1)
where:K545000Aturns,L5lengthofthepart,andD5diameterofthepart(measuredinthesameunitsasthe
length).
(2)Forpartspositionedinthecenterofthecoil:
FIG.4TheEffectiveRegionofInspectionWhenUsinganOffset
CentralConductorisEqualtoFourTimestheDiameterofthe
Conductoras
IndicatedFIG.5EffectiveRegiononInspectionforaLowFill-Factor
CoilFIG.6EffectiveRegionofInspectionforaHigh
Fill-FactorNI5KR~610%!(2)where:R5radiusofthecoil,mm(orin.),K543000AturnsperinchifRismeasuredininches(1690Aturnspermm),L5lengthofthepart,andD5diameterofthepart(measuredinthesameunitsasthelength).Iftheparthashollowportions,replaceDwithDin6.3.7.4.TheseformulasholdonlyifL/Disgreatereffasgiventhan2andlessthan15.IfL/Dislessthan2,polepieces(piecesofferromagneticmaterialwiththesamediameterasthepartbeingtested)shallbeplacedoneachendoftheparttoeffectivelyincreasetheL/Dto2orgreater.IftheL/Disgreaterthan15,thevalueof15shallbesubstitutedforL/D.6.3.7.2LongitudinalMagnetizationwithCableWraporHigh-FillFactorCoils—Whenthecross-sectionalareaofthecoilislessthantwicethecross-sectionalarea(includinghollowportions)ofthepartundertesting,theproductofthenumberofcoilsturns,N,andthecurrentinamperesthroughthecoil,I,shallbeasfollows:NI5K/$~L/D!12%~610%!(3)where:K535000Aturns,L5lengthofthe
part,
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D5diameterofthepart(measuredinthesameunitsasthe
length).
Iftheparthashollowportions,replaceDwithD
6.3.7.4.TheseformulasholdonlyifL/Disgreatereffasgiven
inthan2and
lessthan15.IfL/Dislessthan2,polepieces(piecesof
ferromagneticmaterialwiththesamediameterasthepart
beingtested)shallbeplacedoneachendofthepartto
effectivelyincreasetheL/Dto2orgreater.IftheL/Disgreater
than15,thevalueof15shallbesubstitutedforL/D.
6.3.7.3LongitudinalMagnetizationforIntermediate-Fill
FactorCoils—Whenthecross-sectionalareaofthecoilis
betweentwoandtentimesthecross-sectionalareaofthepart
beinginspected,theproductofthenumberofturns,N,andthe
currentthroughthecoil,I,shallbeasfollows:
NI5~NI!h~102t!/81~NI!l~t22!/8(4)
where:(NI)l5valueofNIcalculatedforlow- llfactorcoilsusing
6.3.7.1,(NI)h5valueofNIcalculatedforhigh- llfactorcoils
t5usingratioof6.3.7.2,thecross-sectionalandareaofthecoiltothe
cross-sectionalareaofthepart(forexample,ifthe
coilis10in.indiameterandthepartisarod5in.
indiameter,t5(p352)/(p32.52)54).
6.3.7.4CalculatingtheL/DRatioforaHolloworCylindri-
calPart—WhencalculatingtheL/Dratioforahollowor
cylindricalpart,Dshallbereplacedwithaneffectivediameter,
Deff,calculatedusingthefollowing:
Deff52@~At2Ah!/p#1/2(5)
where:AAt5totalcross-sectionalofareatheofhollowthepart,portionsand
h5cross-sectionalareaofthepart.
Forcylindricalparts,thisisequaltothefollowing:
Deff5@~OD!22~ID!2#1/2(6)
where:OD5outsidediameterofthecylinder,andID5insidediameterofthecylinder.
6.4ParticleApplication:
6.4.1ContinuousMethod—Inthedrycontinuousmethod,
magneticparticlesareappliedtothepartwhilethemagnetizing
forceispresent.Inthewetcontinuousmethod,themagnetizing
current,orforce,shallbeappliedsimultaneouslywithor
immediatelyafterdivertingthesuspension.Applicationofthe
magneticparticles(see6.4.4and6.4.5)andthemagnetization
methodshallbeasprescribedintheparagraphsreferenced
herein.
6.4.2ResidualMagnetizationMethod—Intheresidualmag-
netizationmethod,themagneticparticlesareappliedtothetest
partimmediatelyafterthemagnetizingforcehasbeendiscon-
tinued.Theresidualmethodisnotassensitiveasthecontinu-
ousmethod,butitcanbeuseful,forexample,indetecting
in-serviceinducedfatiguecracksonthesurfaceofmaterial
withahighretentivity.Itisalsousefulfortheexaminationof
partsinareasinwhich,becauseofgeometricconstraints,thecontinuousmethodcannotbeused.Theresidualmethodshallbeusedonlywhenspeci callyapprovedbythecontractingagencyorwhenithasbeendocumentedthatitcandetectdefectsorarti cialdefectsintestparts.Thetestpartsshallhavethesamematerialandprocessingsteps,andsimilargeometryto,theactualpartsbeinginspected.6.4.3ProlongedMagnetization—Whenusingpolymers,slurries,orpaints,prolongedorrepeatedperiodsofmagneti-zationarenecessarybecauseoflowermagneticparticlemo-bilityinthehigh-viscosityvehicles.6.4.4DryMagneticParticleApplication—Whenusingdryparticles,the owofmagnetizingcurrentshallbeinitiatedpriortoapplicationofthemagneticparticlestothesurfaceundertestingandterminatedafterpowderapplicationhasbeencompletedandanyexcessblownoff.Thedurationofthemagnetizingcurrentshallbeatleast1 2s,andprecautionshallbetakentopreventanydamageofthepartduetooverheatingorothercauses.Drypowdershallbeappliedinamannersuchthatalight,uniform,dust-likecoatingsettlesonthesurfaceofthetestpartwhilethepartisbeingmagnetized.Speciallydesignedpowderblowersorshakersusingcompressedairorhandpowershallbeused.Theapplicatorsshallintroducetheparticlesintotheairinamannersuchthattheyreachthepartsurfaceinauniformcloudwithaminimumofforce.Afterthepowderisapplied,andbeforethemagnetizingforceisre-moved,excesspowdershallberemovedbymeansofadryaircurrentwithsufficientforcetoremovetheexcessparticles,butnotstrongenoughtodisturbparticlesheldbyaleakage eldthatisindicativeofdiscontinuities.Inordertorecognizethebroad,fuzzy,lightlyheldpowderpatternsformedbynear-surfacediscontinuities,theformationofindicationsmustbeobservedcarefullyduringbothpowderapplicationandre-movaloftheexcesspowder.Sufficienttimefortheformationandexaminationofindicationsshallbepermittedduringthetestingprocess.Thedryparticlemethodshallnotbeusedtoinspectaerospacecomponents( ighthardware)withoutspe-ci capprovalofthecontractingagency.6.4.5WetMagneticParticleApplication—Fluorescentornon uorescentparticlessuspendedinaliquidvehicleattherequiredconcentrationshallbeappliedeitherbygentlyspray-ingor owingthesuspensionovertheareatobeinspected.Propersequencingandtimingofpartmagnetizationandapplicationofparticlesuspensionarerequiredtoobtaintheproperformationandretentionofindications.Thisgenerallyrequiresthatthestreamofsuspensionbedivertedfromthepartsimultaneouslywith,orslightlybefore,energizingthemag-neticcircuit.Themagnetizingcurrentshallbeappliedforadurationofatleast1 2sforeachapplication,withaminimumoftwoshotsbeingused.Thesecondshotshouldfollowthe rstinrapidsuccession.Itshouldcomeafterthe owofsuspensionhasbeeninterruptedandbeforethepartisexaminedforindications.Underspecialcircumstances,suchastheuseofautomatedequipmentorforcriticalparts,the1 2-sdurationandthetwo-shotrequirementmaybewaivedprovideditisdemonstratedthatthetestproceduregivenin5.4candetectknowndefectsinrepresentativetestparts.Careshallbeexercisedtopreventanydamagetothepartduetooverheatingorothercauses.Weaklyheldindicationsonhighly
nished
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partsarereadilywashedaway,andhencecaremustbe
exercisedtopreventhigh-velocity owovercriticalsurfaces.
6.4.6MagneticSlurry/PaintApplication—Magneticpaints
orslurriesareappliedtothepartwithabrush,squeezebottle,
oraerosolcanbeforeorduringthemagnetizationoperation.
Thismethodisforspecialapplications,suchasoverheador
underwaterexamination.Thismethodshallbeusedonlywhen
speci callyapprovedbythecontractingagency.
6.4.7MagneticPolymerApplication—Polymerizablemate-
rialcontainingmagneticparticlesshallbeheldincontactwith
thetestpartduringtheperiodofitscure.Beforecuringtakes
place,andwhilethemagneticparticlesarestillmobile,thepart
shallbemagnetizedtothespeci edlevel.Thisrequires
prolongedorrepeatedperiodsofmagnetization.Thismethodis
forspecialapplications,suchasboltholes,whichcannotbe
testedreadilybythewetordrymethod,andshallbeusedonly
whenspeci callyapprovedbythecontractingagency.MIL-I-
83387establishestheinspectionprocessformagneticrubber.
6.5Evaluation—Followingmagnetizationandparticleap-
plication,thepartsshallbeexaminedforindications.All
indicationswillbeidenti edasrelevantornonrelevant.Rel-
evantindicationswillbecomparedtoaccept/rejectcriteriaand
thepartsacceptedorrejectedaccordingly.
6.6RecordingofIndications—Whenrequiredbythewritten
procedure,thelocationofallrejectableindicationsshallbe
markedonthepart,andpermanentrecordsofthelocation,
direction,andfrequencyofindicationsmaybemadebyoneor
moreofthefollowingmethods:
6.6.1WrittenDescription—Byrecordingthelocation,
length,direction,andnumberofindicationsinsketchortabular
form.
6.6.2TransparentTape—Fordryparticleindications,by
applyingtransparentadhesive-backedtapetowhichtheindi-
cationswilladhereandplacingitonanapprovedformalong
withinformationgivingitslocationonthepart.
6.6.3StrippableFilm—Bycoveringtheindicationwitha
spray-onstrippable lmthat xestheindicationsinplaceand
placingtheresultantreproductiononanapprovedformalong
withinformationgivingitslocationonthepart.
6.6.4Photography—Byphotographingorvideorecording
theindicationsthemselves,thetape,orthestrippable lm
reproductionandplacingthephotographinatabularform
alongwithinformationgivingitslocationonthepart.
6.7PostinspectionDemagnetizationandCleaning—Unless
directedotherwisebythecontractingagency,allpartsshallbe
demagnetized,cleaned,andcorrosionprotectedafterexamina-
tion.
6.7.1Demagnetization:
6.7.1.1Whenusingacdemagnetization,thepartshallbe
subjectedtoa eldwithapeakvaluegreaterthan,andinnearly
thesamedirectionas,the eldusedduringexamination.This
ac eldisthendecreasedgraduallytozero.Whenusinganac
demagnetizingcoil,holdthepartapproximately1ft(30cm)in
frontofthecoilandthenmoveitslowlyandsteadilythrough
thecoilandatleast3ft(100cm)beyondtheendofthecoil.
Repeatthisprocessasnecessary.Rotateandtumblepartsof
complexcon gurationwhilepassingthroughthe eldofthe
coil.6.7.1.2Whenusingdcdemagnetization,theinitial eldshallbehigherthan,andinnearlythesamedirectionas,the eldreachedduringexamination.The eldshallthenbereversed,decreasedinmagnitude,andtheprocessrepeated(cycled)untilanacceptablylowvalueofresidual eldisreached.6.7.1.3Wheneverpossible,partsthathavebeenmagnetizedcircularlyshallbemagnetizedinthelongitudinaldirectionbeforebeingdemagnetized.Afterdemagnetization,amagnetic eldprobeorstrengthmetershallnotdetect eldswithanabsolutevalueabove3G(240Am 1)anywhereonthepart.6.7.2PostinspectionCleaning—Cleaningshallbedonewithasuitablesolvent,airblower,orbyothermeans.Partsshallbeinspectedtoensurethatthecleaningprocedurehasremovedmagneticparticleresiduesfromcoolantholes,crev-ices,passageways,etc.,sincesuchresiduecouldhaveanadverseeffectontheintendeduseofthepart.Careshallbetakentoremoveallplugs,masking,orotherprocessingaidsthatmayaffecttheintendeduseofthepart.Partsshallbeprotectedfromanypossiblecorrosionordamageduringthecleaningprocessandshallbetreatedtopreventtheoccurrenceofcorrosionafter nalinspection.7.QualityControl7.1SystemPerformance:7.1.1SystemPerformanceVeri cation—Theoverallperfor-manceofthemagneticparticleexaminationsystem,includingtheequipment,materials,andthelightingenvironmentbeingused,shallbeveri edinitiallyandatregularintervalsthere-after.Therequiredveri cationintervalsarestatedinTable1.Recordsoftheveri cationresultsshallbemaintainedandretainedforthetimeperiodspeci edinthecontract.Frequencyofcalibrationforcurrentandvoltagemeasuringdevices,ammetershunts,timers,andgaussmetersusedintheveri ca-tionshallcomplywiththerequirementsofMIL-STD-45662orTable1,asspeci edbythecognizantLevelIII.7.1.2UseofTestPartswithDiscontinuities—Areliablemethodforinspectionsystemveri cationistheuseofrepre-sentativetestpartscontainingdefectsofthetype,location,andsizespeci edintheacceptancerequirements.Ifcorrectmag-neticparticleindicationscanbeproducedandidenti edintheserepresentativeparts,theoverallsystemandinspectionprocedureisveri ed.Partsusedforveri cationwillbedemagnetized,cleanedthoroughlyfollowingtheexamination,andcheckedunderblackorvisiblelight,asappropriatetotheexaminationprocess,toensurethatresidualindicationsdonotremain.7.1.3FabricatedTestPartswithArti cialDiscontinuities—Whenactualproductionpartswithknowndiscontinuitiesofthetype,location,andsizeneededforveri cationarenotavailableorareimpractical,fabricatedtestpartswitharti cialdisconti-nuitiesshallbeused.Arti cialdiscontinuitiesmaybefabri-catedtomeetaparticularneedormaybecommerciallyavailablemagnetic eldindicatorsorshimsasshowninFig.2andFig.7.Allapplicableconditionsfortheuseofsuchtestparts,asdescribedin7.1.2,shallapply.Whencommercialdevicesareused,theirmagneticproperties, awtypes,andsurfaceconditionshallbeasclosetotheproductionpartas
possible.
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FIG.7Pie- eldIndicatorforUseinMagneticParticleInspection
SystemVeri cation(AllDimensionsarein
Inches)
7.1.4SuspensionVehicleTests(Notrequiredforaerosol
cansolutions):
7.1.4.1Concentration/ContaminationTests—Particlecon-
centrationandcontaminationshallbedetermineduponstart
up,atregularintervalsthereafter,andwheneverthebathis
changedoradjusted.Therequiredtestingintervalsarestatedin
Table1.
(1)DeterminationofWetParticleConcentration—Agitate
theparticlesuspensionaminimumof30mintoensureuniform
distributionofparticlesthroughoutthebath.Placea100-mL
sampleoftheagitatedsuspensioninapear-shapedcentrifuge
tube(ofthesizeandshapespeci edinTestMethodsD96,
exceptgraduatedto1mLin0.05-mLincrements).Demagne-
tizethesampleandallowthetubetostandundisturbedforat
least60minifusingthepetroleumdistillateinAMS2641or
30minsettlingtimeforconditionedwatersuspension.Read
thevolumeofsettledparticles.Iftheconcentrationisoutofthe
tolerancestatedinthewrittenprocedure(orthatgivenin
5.8.5),addtheparticlesorsuspensionvehicle,asrequired,and
redeterminetheparticleconcentration.Ifthesettledparticles
appeartobelooseagglomeratesratherthanasolidlayer,take
asecondsample.Ifthesecondsamplealsoappearsagglomer-
ated,replacetheentiresuspension.Thirty-minutesettling
times,orotheracceleratedtests,maybeusediftheyhavebeen
veri edtogiveresultsequivalenttotheproceduredescribedin
thisparagraph.
(2)DeterminationofWetParticleContamination—Perform
thetestsspeci edin7.1.4.1(1).Inaddition,for uorescent
baths,examinetheliquidabovetheprecipitatewithblacklight.
Theliquidshallbecomparabletothe uorescenceofthe
originalsolution.Examinethegraduatedportionofthetube,
underbothblacklight(for uorescentbathsonly)andvisible
light(forboth uorescentandnon uorescentbaths),for
striationsorbands,differentincolororappearance.Bandsor
striationsmayindicatecontamination.Ifthetotalvolumeofthecontaminants,includingbandsorstriations,exceeds30%ofthevolumeofmagneticparticles,oriftheliquidisnoticeably uorescent,thebathmustbereplaced.7.1.4.2WaterBreakTest—Inthistestofwater-basedve-hicles,acleanpartwithasurface nishthesameasthepartstobetestedis oodedwiththeconditionedwater,andtheappearanceofthesurfaceisnotedafter oodingisstopped.Ifacontinuouseven lmformsovertheentirepart,sufficientwettingagentispresent.Ifthe lmofsuspensionbreaks,exposingbaresurface,insufficientwettingagentispresentortheparthasnotbeencleanedadequately.7.1.5EquipmentCalibration—MagneticparticletestingequipmentshallbecheckedforperformanceandaccuracyatthetimeofpurchaseandatintervalsthereafterasgiveninTable1,whenevermalfunctionissuspectedorwhenspeci edbythecontractingagency,andwheneverelectricalmainte-nancethatmightaffectequipmentaccuracyisperformed.7.1.5.1AmmeterAccuracy—Tochecktheequipmentam-meter,parativereadingsshallbetakenatthreeoutputlevelsencompassingtheuseablerangeoftheequip-ment.Theequipmentmeterreadingshallnotdeviatebymorethan610%offullscalefromthecurrentvalueshownbythecalibratedammeter.(Whenmeasuringhalf-wavealternatingcurrent,thecurrentvaluesshownbythecalibrateddcammeterreadingsshallbedoubled.)Thefrequencyoftheammetercheckisspeci edinTable1.7.1.5.2TimerControlCheck—Onequipmentusingatimertocontrolthecurrentduration,thetimershouldbecheckedtowithin60.1susingasuitableelectronictimer.7.1.5.3MagneticFieldQuickBreakCheck—Onequipmentthatusesaquickbreakfeature,properfunctioningofthiscircuitshallbeveri ed.Thetestmaybeperformedusingasuitableoscilloscopeorotherapplicablemethodasspeci edbytheequipmentmanufacturer.7.1.5.4DeadWeightCheck—Yokesandpermanentmagnet-ics(whenallowed)shallbedeadweighttestedatintervalsasstatedinTable1.Alternatingcurrentyokesshallhavealiftingforceofatleast10lb(45N),witha2to4-in.(50to100-mm)spacingbetweenlegs.Directcurrentyokesshallhavealiftingforceofatleast30lb(135N),witha2to4-in.(50to100-mm)spacingbetweenlegs,or50lb(225N),witha4to6-in.(100to150-mm)spacing.7.2MarkingofInspectedParts—Unlessotherwisespeci edbythecontractingagency,partsthathavebeenacceptedusingmagneticparticleexaminationshallbemarkedinaccordancewiththeapplicabledrawing,purchaseorder,contract,orasspeci edherein.Markingshallbeappliedinsuchamannerandlocationastobeharmlesstothepart.Theidenti cationshallnotbeobliteratedorsmearedbysubsequenthandlingand,whenpracticable,placedinalocationthatwillbevisibleafterassembly.Whensubsequentprocessingwouldremovetheidenti cation,theapplicablemarkingshallbeaffixedtotherecordaccompanyingthe nishedpartsorassembly.Boltsandnutsandotherfastenerproductsmaybeidenti edashavingmettherequirementsofmagneticparticleexaminationbymarkingeachpackageconspicuously.7.2.1ImpressionStamping,InkStamping,Laser
Marking,
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orVibroEngraving—Impressionstamping,inkstamping,laser
marking,orvibroengravingshallbeusedwhenpermittedor
requiredbytheapplicablewrittenprocedure,detailspeci ca-
tionordrawing,orwhenthenatureofthepartissuchasto
provideforimpressionstampingofpartnumbersorother
inspector’smarkings.Impressionstampingshallbelocated
onlyintheareaprovidedadjacenttothepartnumberor
inspector’sstampunlessotherwisespeci edbythecontracting
agency.
7.2.2Etching—Whenimpressionstamping,inkstamping,
lasermarking,orvibroengravingisprohibited,partsshallbe
etchedusinganetching uidorothermeansandamethodof
applicationacceptabletothecontractingagency.Theetching
processandlocationshallnotaffectthefunctioningofthepart
adversely.
7.2.3Dyeing—Whenstamping,vibroengraving,oretching
isnotpermissible,identi cationshallbeaccomplishedby
dyeing.
7.2.4OtherIdenti cation—Othermeansofidenti cation,
suchastagging,shallbeusedforpartsthathaveaconstruction
orfunctionprecludingtheuseofstamping,vibroengraving,or
etching,asinthecaseofcompletelygroundorpolishedballs,
rollers,pins,orbushings.
7.2.5IdentifyingSymbolsandColorMarkings:
7.2.5.1One-HundredPercentExamination—Whenitems
areexaminedandacceptedby100%examination,eachitem
shallbemarkedasfollows:
(1)Dyeing—Whendyeingisapplicable,adyeofacceptable
adherencewhichispredominantlyblue(perFED-STD-595)
shallbeemployed.However,ifacolorcon ictisincurredwith
anyothermethod,magneticparticleexaminationcanbe
indicatedbytwoadjacentbluedotsorothersuitablemeans.
(2)Stamping,LaserMarking,VibroEngraving,or
Etching—Whenimpressionstampingorinkstamping,laser
marking,vibroengraving,oretchingisusedtomark100%
inspectedparts,theletter“M”withacirclearounditwillbe
employed.
7.2.5.2LotInspection—Whenitemsareacceptedbymeans
ofasamplingprocedure,eachitemofanacceptedlotshallbe
markedasfollows:
(1)Dyeing—Whendyeingisapplicable,adyeofacceptable
adherencethatispredominantlyorange(perFED-STD-595)
shallbeemployed.(2)Stamping,VibroEngraving,orEtching—Whenimpres-sionstamping,vibroengravingoretchingisusedtomarklotinspectedparts,theletter“M”shallbeemployed.7.3EyeGlasses—Whenusing uorescentmaterials,inspec-torsshallnotweareyeglassesthatarephotochromicorthathavepermanentlydarkenedlenses.Thisisnotintendedtoprohibittheuseofeyeglasseswithlensestreatedtoabsorbultravioletlight.7.4Safety—Thesafehandlingofmagneticparticles(wetordry),oilvehicleswaterbaths,andwaterconditionerconcen-tratesaregovernedbythesuppliers’MaterialSafetyDataSheets(MSDS).MaterialSafetyDataSheets,conformingto29CFR1910.1200,orequivalent,mustbeprovidedbythesuppliertoanyuserandshallbepreparedinaccordancewithFED-STD-313.7.4.1Flammability—FlashpointofoilvehiclesshallbeinaccordancewithAMS2641orDoD-F-87935.Thesuppliers’MSDSshallcertifythe ashpoint.7.4.2PersonnelHazards—Precautionsagainstinhalation,skincontact,andeyeexposurearedetailedinthesuppliers’MSDS.Theseprecautionsshallbeobserved.7.4.3ElectricalHazards—Magnetizingequipmentshallbemaintainedproperlytopreventpersonnelhazardsfromelec-tricalshortcircuits.Caremustbetakentoreducearcingandthepossibleignitionofoilbaths.7.4.4BlackLight—Itisrecommendedthattheintensityofblacklightincidentonunprotectedskinoreyesnotexceed1000µW/cm2.Crackedorbrokenultraviolet ltersshallbereplacedimmediately.Brokenbulbscancontinuetoradiateultravioletenergyandmustbereplacedimmediately.Spec-taclesdesignedtoabsorbultravioletwavelengthradiationaresuggestedforclose,high,blacklightintensityexamination.7.5DarkAdaptation—Personnelmustwaitatleast1minafterenteringadarkenedareafortheireyestoadjusttothelow-levellightingbeforeperforming uorescentmagneticparticleexamination.8.Keywords8.1dye; uorescent;magneticparticle;nondestructiveevaluation;nondestructiveexamination;nondestructive
testing
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APPENDIX
(NonmandatoryInformation)
X1.MEASUREMENTOFTANGENTIALFIELDSTRENGTH
X1.1Caremustbeexercisedwhenmeasuringthetangen-
tialapplied eldstrengthsspeci edin6.3.2.Theactiveareaof
theHalleffectprobeshouldbenolargerthan0.2in.(5mm)by
0.2in.(5mm)andshouldhaveamaximumcenterlocation5
mmfromthepartsurface.Theplaneoftheprobemustbe
perpendiculartothesurfaceofthepartatthelocationof
measurementtowithin5degrees.Thisisdifficulttoaccom-
plishbyhandorientation,thereforetheprobeshouldbeheldin
ajigor xtureofsometype.Ifthecurrentisbeingappliedin
shots,orifalternatingcurrentorhalf-waverecti edalternatingcurrentisbeingused,thegaussmetershouldbesettoreadthepeakvalueduringtheshot.Thegaussmetershouldhaveafrequencyresponseof0to300Hzorhigher.Thedirectionandmagnitudeofthetangential eldonthepartsurfacecanbedeterminedbytwomeasurementsmadeatrightanglestoeachotheratthesamespot.Thegaussmeterprobeleadsshouldbeshieldedortwistedtopreventreadingerrorsduetovoltageinducedduringthelarge eldchangesencounteredduringmagneticparticleexamination.
ersofthisstandardareexpresslyadvisedthatdeterminationofthevalidityofanysuchpatentrights,andtheriskofinfringementofsuchrights,areentirelytheirownresponsibility.
Thisstandardissubjecttorevisionatanytimebytheresponsibletechnicalcommitteeandmustbereviewedevery veyearsandifnotrevised,eitherreapprovedorwithdrawn.YourcommentsareinvitedeitherforrevisionofthisstandardorforadditionalstandardsandshouldbeaddressedtoASTMHeadquarters.Yourcommentswillreceivecarefulconsiderationatameetingoftheresponsibletechnicalcommittee,whichyoumayattend.IfyoufeelthatyourcommentshavenotreceivedafairhearingyoushouldmakeyourviewsknowntotheASTMCommitteeonStandards,100BarrHarborDrive,WestConshohocken,PA19428.
ThisstandardiscopyrightedbyASTM,100BarrHarborDrive,WestConshohocken,PA19428-2959,UnitedStates.Individualreprints(singleormultiplecopies)ofthisstandardmaybeobtainedbycontactingASTMattheaboveaddressorat610-832-9585(phone),610-832-9555(fax),orservice@(e-mail);orthroughtheASTMwebsite
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